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doi: 10.1095/biolreprod.116.142877 15 GouY.LiX.LiP.ZhangH.XuT.WangH.et al

The sample (10 l) was injected into an Agilent 1260 Infinity LC system attached to an Agilent 6120 Single Quadrupole MS with ESI source and evaporative light scattering detector (ELSD)