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Liquid Chromatography and Gas Chromatography Mass Spectrometry LC-MS measurements were conducted on a Waters ACQUITY ultra-performance liquid chromatograph (UPLC) and a ThermoFisher Scientific Orbitrap Elite high resolution/accurate mass spectrometer (Thermo Scientific, Waltham, MA, USA), which consisted of a heated electrospray ionization (HESI) source and orbitrap mass analyzer operated at a resolution 30,000 mass